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1129 sunflower oil specifications.

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Applies to sunflower oil intended for direct consumption, production food products, including for baby food, and industrial processing.

3 Terms and definitions

4 Classification

5 Technical requirements

7 Acceptance rules

8 Control methods

10 Expiration dates

Annex A (informative) Fatty acid composition of sunflower oil

Annex B (informative) Norms and method of monitoring the indicator " mass fraction unsaponifiable substances" in sunflower oil

Annex E (mandatory) Cold test

This GOST is in:

Organizations:

07.06.2013	Approved	43
28.10.2013	Approved	1253-st-st
	Published	2014
	Designed

sunflower oil. Specifications

Normative references

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INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION

INTERSTATE

STANDARD

SUNFLOWER OIL

Specifications

Official edition

Standartinform

Foreword

The goals, basic principles and basic procedure for carrying out work on interstate standardization are established by GOST 1.0-92 “Interstate standardization system. Basic Provisions” and GOST 1.2-2009 “Interstate Standardization System. Interstate standards, rules and recommendations for interstate standardization. Rules for the development, adoption, application, updating and cancellation "

About the standard

1 PREPARED by the State Scientific Institution "All-Russian Research Institute of Fats of the Russian Academy of Agricultural Sciences" (GNU "VNIIZH" of the Russian Agricultural Academy)

2 INTRODUCED by the Federal Agency for Technical Regulation and Metrology (TK238)

3 ADOPTED by the Interstate Council for Standardization, Metrology and Certification (Minutes of June 7, 2013 No. 43)

4 This standard complies with the following international standard and international document:

ISO 6885:1998(E) Animal and vegetable fats and oils - Determination ofanisidine value (Annex E);

AOCS Official Method Cc 11-53 Cold Test

The degree of conformity is non-equivalent (NEQ).

This standard has been prepared based on the application of GOST R 52465-2005

5 By order of the Federal Agency for Technical Regulation and Metrology dated October 28, 2013 No. 1253-st, the interstate standard GOST 1129-2013 was introduced as a national standard Russian Federation since July 1, 2014

6 INTRODUCED FOR THE FIRST TIME

Information about changes to this standard is published in the annual information index "National Standards", and the text of changes and amendments - in the monthly information index "National Standards". In case of revision (replacement) or cancellation of this standard, a corresponding notice will be published in the monthly information index "National Standards". Relevant information, notification and texts are also placed in information system general use - on the official website of the Federal Agency for Technical Regulation and Metrology on the Internet

©Standartinform, 2014

In the Russian Federation, this standard cannot be fully or partially reproduced, replicated and distributed as an official publication without the permission of the Federal Agency for Technical Regulation and Metrology

8.17 Determination of mycotoxins - according to GOST 30711.

8.18 Determination of strontium-90, cesium-137 - according to normative document operating in the territory of the state that adopted the standard.

8.19 Determination of microbiological indicators - according to the regulatory document in force in the territory of the state that adopted the standard.

9 Transport and storage

9.1 Sunflower oil is transported by all modes of transport in accordance with the requirements of the legislation on technical regulation and the terms of the contract for the supply of products.

9.2 Bulk sunflower oil is transported in railway tanks equipped with a bottom drain, in tankers with tightly closed hatches and other covered vehicles in accordance with the requirements of the legislation on technical regulation and the terms of the contract for the supply of products.

When transporting by open vehicles, barrels, flasks and boxes with packaged sunflower oil must be protected from precipitation and sunlight.

9.3 Shipment of consumer containers with sunflower oil in open boxes must be agreed with the consumer.

9.4 Sunflower oil in consumer packaging, packed in corrugated cardboard boxes and grouped in shrink film, is transported in railway cars on pallets. The placement and fastening of boxes, transport packages and group packages must comply with the requirements of GOST 22477.

9.5 It is allowed to stack the boxes on pallets fixed on the walls of the car with the help of fasteners and wooden skids. The stacking height of boxes on pallets should not exceed five tiers.

9.6 Rail tank cars and tank trucks must comply with the requirements for the transport of food products.

Pouring sunflower oil intended for direct consumption into railway tanks and tank trucks is carried out using a pipeline reaching the bottom of the tank.

9.7 Transportation of barrels, flasks, as well as boxes with packaged sunflower oil in transport packages is carried out in accordance with the requirements of GOST 21650, GOST 22477, GOST 24597 and GOST 26663.

9.8 Sunflower oil before being poured into railway tanks and tankers, into flasks and barrels, before being filled into consumer packaging, is stored under conditions that ensure its safety within the limits of the indicators of this brand of oil.

Sunflower oil packaged in consumer containers is stored in covered darkened rooms, in flasks and barrels - in covered areas.

10 EXPIRY DATES

10.1 The shelf life of sunflower oil is set by the manufacturer depending on the production technology and storage conditions in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.

Annex A (informative)

Fatty acid composition of sunflower oil

A.1 The fatty acid composition of sunflower oil is given in Table A.1.

Table A.1

Fatty acid name	Mass fraction of fatty acid (%, to the amount of fatty acids)
Ci4;o Tetradecanoic (myristic)
Ci6:o Hydroxydecanoic (palmitic)
Ci6:i Hexadecene (Palmitoleic)
Cis;o Octadecanic (stearic)



C 2 o: o Eicosanoic (arachidic)
C 2 o:i Eicosene (gondoic)
O 22: O Docosan (behenic)
C 22: i Docosane (erucic)
From 24; o Tetracosanoic (lignoceric)

Determination of fatty acid composition - according to GOST 30418 and GOST 31663.

Annex B (informative)

Norms and method of control of the indicator "mass fraction of unsaponifiable substances"

in sunflower oil

B.1 The norms and method of monitoring the indicator "mass fraction of unsaponifiable substances" in sunflower oil are given in Table B.1.

Determination of the mass fraction of unsaponifiable substances - according to GOST 5479.

Calculation of the energy value of vegetable oil

Energy value, kcal / 100 g, is calculated by the formula

Energy value = 9 (100 - W - N),

where 9 is the coefficient of energy value for fats, kcal / g - by,

W- mass fraction of moisture and volatile substances,%, - according to GOST 11812.

N - mass fraction of non-fat impurities,%, - according to GOST 5481.

D.1 Glass bottles with sunflower oil are packed in wooden reusable boxes according to GOST 10131 (No. 18,26,27) and GOST 11354, as well as plastic reusable boxes for bottles according to the document in accordance with which they are made, and corrugated cardboard boxes according to GOST 13511.

Glass bottles are packed in wire reusable boxes according to the document in accordance with which they are manufactured, as well as in containers-equipment in accordance with GOST 24831 only for local sale.

D.2 Packages with sunflower oil are packed in corrugated cardboard boxes No. 9 according to GOST 13511.

D.3 Bottles from polymer materials with sunflower oil are packed in corrugated cardboard boxes in accordance with GOST 9142 and GOST 13516 or other boxes according to the document in accordance with which they are made, ensuring the safety of products, or they are formed for packaging in shrink film in accordance with GOST 25951 or other film with similar properties according to the document according to which it is manufactured. Group packaging is formed using trays or pads made of corrugated cardboard according to GOST 7376, or cardboard for consumer packaging according to GOST 7933, or without gaskets. Group packaging is carried out in accordance with the requirements of GOST 25776.

D.4 If necessary, products packed in shrink film are formed into bags on flat pallets in accordance with GOST 9078 or GOST 26381. To fasten packages into a bag, polyethylene film is used according to GOST 10354, steel tape according to GOST 3560, polypropylene tape or stretch film according to the document in accordance with which they are made.

Palletizing is carried out in accordance with the requirements of GOST 22477, GOST 23285 and GOST 24597.

When forming transport packages using a shrink film, it is not allowed to weld it with a group packaging film.

D.5 Bulk sunflower oil is poured into aluminum flasks according to GOST 5037 with sealing rings made of oil-resistant rubber according to GOST 17133 and other materials approved for contact with vegetable oils in in due course, in non-galvanized steel barrels for foodstuffs in accordance with GOST 13950, in barrels made of polymeric materials approved for contact with vegetable oils in the prescribed manner, in railway tanks and tankers, and also, in agreement with the consumer, in other types of containers that ensure the safety of products and made from materials approved for contact with vegetable oils in the prescribed manner.

It is allowed to use other equipment with technical and metrological characteristics not worse and reagents in quality not lower than those indicated.

E.4 Preparation for determination

E.5 Conducting a determination

E.5.2 The flask with the analyzed oil sample, prepared according to D.5.1, is placed in a water bath with ice so that the contents of the flask are completely covered with ice water, and kept for 5.5 hours at a temperature of 0 °C, periodically adding ice to maintain the specified temperature.

After that, the flask with the analyzed oil sample is removed from the water bath and visually inspected for the presence of fat crystals or turbidity, taking care not to mistake small dispersed air bubbles for fat crystals. It is recommended to view the analyzed oil sample against a dark background at a distance of about 2 m from the dark background.

The test is considered positive if the analyzed oil sample is completely transparent (the test is passed).

If necessary, the test is continued for more than 5.5 hours. In this case, the analyzed oil sample is tested every hour, returning after each inspection to the ice water bath as quickly as possible so that the temperature of the oil does not increase.

GOST 1129-2013

1 area of use............................................... ....one

3 Terms and definitions .......................................................... ..3

4 Classification................................................... ......3

5 Specifications .................................................................. .4

6 Environmental requirements ............................................................... 7

7 Rules for acceptance ............................................... ......7

8 Methods of control ............................................... ......7

9 Transport and storage...............................................................8

10 Expiration dates............................................................... .......eight

Annex A (informative) Fatty-acid composition of sunflower oil ..................9

Annex B (informative) Norms and method of monitoring the indicator "mass fraction of unsaponifiable

substances” in sunflower oil .............................................. 10

Annex E (mandatory) Cold test .........................................13

Bibliography................................................. .......fifteen

INTERSTATE STANDARD

SUNFLOWER OIL Specifications

sunflower oil. Specifications

Introduction date - 2014-07-01

1 area of use

This standard applies to sunflower oil intended for direct human consumption, food production, including baby food, and industrial processing.

Requirements ensuring product safety - in 5.2.1-5.2.3, 5.3.2, product quality requirements - in 5.1,5.2.3, 5.3.1, labeling requirements - in 5.4.

2 Normative references

This standard uses Normative references to the following interstate standards:

5.4 Marking

5.4.1 Each packaging unit of sunflower oil in a consumer container (label or package) is marked by any method that ensures its clear identification, indicating:

Product name;

Name and location of the manufacturer (address indicating the country of manufacture) or address of the organization authorized by the manufacturer to accept claims from purchasers;

Net weight and/or product volume;

Trademark of the manufacturer (if any);

Product brands;

Production dates (bottling dates for the packaged product);

Nutritional value (fat content in 100 g of oil);

Energy value of 100 g of the product, kcal (according to Appendix B);

Expiry date;

The designations of this standard;

Information on confirmation of conformity;

The date of manufacture (bottling date) of sunflower oil is applied in any way that ensures its clear reading.

5.4.2 Each unit of transport container with sunflower oil is marked with:

Name and location ( legal address a) manufacturer or packer;

Product name;

Product brand;

Net weight and number of consumer packaging units in a packaging unit for packaged oil or net weight of bulk oil;

Lot number and/or packing unit number;

Date of manufacture (date of pouring bulk sunflower oil in barrels, flasks, cisterns, tanks, containers or date of pouring packaged sunflower oil in consumer packaging);

Trademark of the manufacturer (if any);

Shelf life;

Names and designations of this standard;

Information about conformity assessment;

When grouped in shrink film, additional labeling characterizing the product is not required.

Open boxes for packing oil bottles are not labelled.

5.4.3 Handling signs “Keep out of sunlight”, “Keep out of moisture”, “Top” and “Fragile. Caution" is applied in accordance with GOST 14192.

Additional requirements for transport marking must comply with the terms of the contract for the supply of products.

5.4.4 When supplying sunflower oil for export, the marking must comply with the requirements of foreign trade organizations.

5.5 Packaging

5.5.1 Sunflower oil is produced packaged and bulk.

5.5.2 Sunflower oil is packaged by weight or volume in any consumer packaging made from materials approved for contact with vegetable oils in the prescribed manner. When packaging sunflower oil for baby food, it is necessary to additionally take into account the requirements established by regulatory legal acts in force in the territory of the state that adopted the standard.

Limits of permissible negative deviations of the net content from the nominal quantity according to GOST 8.579.

5.5.3 Consumer containers with sunflower oil are hermetically sealed with caps, plugs or lids made of materials approved for contact with vegetable oils.

6 Environmental requirements

6.1 Control of maximum permissible concentrations (MPC) of harmful substances in the air is carried out in accordance with GOST 17.2.3.02 and with regulatory legal acts in force on the territory of the state that adopted the standard.

6.2 Soil protection from pollution by household and industrial waste is carried out in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.

6.3 Wastewater treatment, water consumption and water disposal in the production of sunflower oil is carried out in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.

7 Acceptance rules

7.2 Each batch of sunflower oil must be checked by the manufacturer's laboratory for compliance with the requirements of this standard and issued with a certificate of quality and safety.

7.3 Control over the content of toxic elements, pesticides, mycotoxins and radionuclides, as well as microbiological indicators of sunflower oil intended for baby food, is carried out in accordance with the procedure established by the product manufacturer and guaranteeing product safety.

7.4 The manufacturer guarantees compliance with the standards in terms of "cold test" and "anisidine number" on the basis of periodic analyzes carried out at least once a month.

8 Control methods

8.1 Sampling method - according to GOST 5471 .. Containers made of cardboard and combined materials for food products. Specifications.

GOST R 53228-2008 Scales of non-automatic action. Part 1. Metrological and technical requirements. Tests.

INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ICC)

INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC)

GOST 1129-2013

INTERSTATE STANDARD

SUNFLOWER OIL

Specifications

Official edition

Moscow Standard inform 2014

GOST 1129-2013

Foreword

About the standard

1 PREPARED by the State Scientific Institution "All-Russian Research Institute of Fats of the Russian Academy of Agricultural Sciences" (GNU "VNIIZH" of the Russian Agricultural Academy)

2 INTRODUCED by the Federal Agency for Technical Regulation and Metrology (TK 238)

3 ADOPTED by the Interstate Council for Standardization, Metrology and Certification (Minutes of June 7, 2013 No. 43)

4 This International Standard conforms to the following International Standard and International Document:

ISO 6885:1998(E) Animal and vegetable fatsand oils - Determination of anisidine value

AOCS Official Method Cc 11-53 Cold Test

The degree of conformity is non-equivalent (NEQ).

This standard has been prepared based on the application of GOST R 52465-2005

5 By order of the Federal Agency for Technical Regulation and Metrology dated October 28, 2013 No. 1253-st, the interstate standard GOST 1129-2013 was put into effect as the national standard of the Russian Federation from July 1, 2014.

6 INTRODUCED FOR THE FIRST TIME

Information about changes to this standard is published in the annual information index "National Standards", and the text of changes and amendments - in the monthly information index "National Standards". In case of revision (replacement) or cancellation of this standard, a corresponding notice will be published in the monthly information index "National Standards". Relevant information, notification and texts are also posted in the public information system - on the official website of the Federal Agency for Technical Regulation and Metrology on the Internet

©Standartinform.2014

1 area of use

3 Terms and definitions

4 Classification

5 Technical requirements

7 Acceptance rules

8 Control methods

10 Expiration dates

Annex A (informative) Fatty acid composition of sunflower oil

Annex B (informative) Standards and method for monitoring the indicator "mass fraction of unsaponifiable substances" in sunflower oil

Annex E (mandatory) Cold test

Bibliography

INTERSTATE STANDARD

SUNFLOWER OIL

Specifications

sunflower oil. Specifications

Introduction date - 2014-07-01

1 area of use

This standard applies to sunflower oil intended for direct human consumption, food production, including baby food, and industrial processing.

Requirements ensuring product safety - in 5.2.1-5.2.3, 5.3.2, product quality requirements - in 5.1,5.2.3,5.3.1, labeling requirements - in 5.4.

This standard uses normative references to the following interstate standards:

GOST 8.579-2002 State system ensuring the uniformity of measurements. Requirements for the quantity of packaged goods in packages of any kind during their production, packaging, sale and import

GOST 12.1.007-76 Occupational safety standards system. Harmful substances. Classification and general safety requirements

GOST 12.1.018-93 Occupational safety standards system. Fire and explosion safety static electricity. General requirements

GOST 12.1.019-79 Occupational safety standards system. Electrical safety. General requirements and nomenclature of types of protection

GOST 17.2.3.02-78 Nature protection. Atmosphere. Rules for establishing permissible emissions of harmful substances industrial enterprises

GOST 61-75 Reagents. Acetic acid. Specifications

GOST 1770-74 (ISO 1042-83, ISO 4788-80) Measuring laboratory glassware. Cylinders, beakers, flasks, test tubes. General specifications

GOST 3560-73 Steel packing tape. Specifications

GOST 4166-76 Reagents. Sodium sulfate. Specifications

GOST 4453-74 Powdered wood brightening active charcoal. Specifications

GOST 5037-97 Metal flasks for milk and dairy products. Specifications

GOST 5471-83 Vegetable oils. Acceptance rules and sampling methods

GOST 5472-50 Vegetable oils. Determination of smell, color and transparency

GOST 5476-80* Vegetable oils. Methods for determining acid number

GOST 5477-93 Vegetable oils. Methods for determining color

* GOST R52110-2003 Vegetable oils. Methods for determining the acid number.

Official edition

GOST 5479-64 Vegetable oils and natural fatty acids. Method for determination of unsaponifiable substances

GOST 5480-59 Vegetable oils and natural fatty acids. Methods for the determination of soap GOST 5481-89 Vegetable oils. Methods for determination of non-fat impurities and sludge GOST 5644-75 Anhydrous sodium sulfite. Specifications

GOST 6709-72 Distilled water. Specifications

GOST 7376-89 1 Corrugated cardboard for product packaging. Specifications

GOST 7933-89 Cardboard for consumer packaging. General specifications

GOST 9078-84 Flat pallets. General specifications

GOST 9142-90 Corrugated cardboard boxes. General specifications

GOST 9287-59 Vegetable oils. Method for determining the flash point in a closed cup

GOST 10131-93 Boxes made of wood and wood materials for food industry products, Agriculture and matches. Specifications

GOST 10354-82 Polyethylene film. Specifications

GOST 11354-93 Reusable boxes made of wood and wood materials for products of the food industry and agriculture. Specifications

GOST 11812-66 Vegetable oils. Methods for determining moisture and volatile substances

GOST 12026-76 Laboratory filter paper. Specifications

GOST 13511-2006 Corrugated cardboard boxes for food products, matches, tobacco products and detergents. Specifications

GOST 13516-86 2 Corrugated cardboard boxes for canned food, preserves and food liquids. Specifications

GOST 13950-91 Welded steel barrels and rolling barrels with corrugations on the body. Technical conditions GOST 14192-96 Cargo marking

GOST 14919-83 Household electric stoves, electric stoves and ovens. General specifications

GOST 15846-2002 Products shipped to the Far North and equivalent areas. Packaging, marking, transportation and storage

GOST 17133-83 Rubber plates for products in contact with food. Specifications

GOST 21650-76 Means of fastening packaged cargoes in overpacks. General requirements

GOST 22391-89 Sunflower. Procurement and delivery requirements

GOST 22477-77 Means of fastening transport packages in covered wagons. General technical requirements

GOST 23285-78 Transport bags for foodstuffs and glass containers. Specifications

GOST 23683-89 Petroleum solid paraffins. Specifications

GOST 24104-200G 2 Laboratory balances. General technical requirements

GOST 24597-81 Packages of packaged goods. Main parameters and dimensions

GOST 24831-81 Packaging equipment. Types, basic parameters and dimensions

GOST 25336-82 Laboratory glassware and equipment. Types, basic parameters and dimensions

GOST 25776-83 Piece products and in consumer packaging. Group packaging in shrink film

GOST 25951-83 Polyethylene shrink film. Specifications

GOST 26381-84 Single-use flat pallets. General specifications GOST 26593-85 Vegetable oils. Method for determining peroxide value

GOST 26663-85 Transport packages. Formation using packaging tools. General technical requirements

GOST 26927-86 Food raw materials and products. Mercury determination method

GOST 26929-94 Food raw materials and products. Sample preparation. Mineralization to determine the content of toxic elements

GOST 26930-86 Food raw materials and products. Arsenic determination method

GOST 26932-86 Food raw materials and products. Lead determination methods

GOST 26933-86 Food raw materials and products. Methods for the determination of cadmium

GOST 28498-90 Liquid glass thermometers. General technical requirements. Test Methods

GOST 29169-91 (ISO 648-77) Laboratory glassware. Pipettes with one mark

GOST 30178-96 Food raw materials and products. Atomic absorption method for the determination of toxic elements

GOST 30418-96 Vegetable oils. Method for determination of fatty acid composition

GOST 30538-97 Food products. Method for determining toxic elements by atomic emission method

GOST 30711-2001 Food products. Methods for the detection and determination of the content of aflatoxins B 1 and M,

GOST 31663-2012 Vegetable oils and animal fats. Determination by gas chromatography of the mass fraction of methyl esters of fatty acids

GOST 31628-2012 Food products and food raw materials. Stripping voltammetric method for determining the mass concentration of arsenic

GOST 31753-2012 Vegetable oils. Methods for the determination of phosphorus-containing substances

GOST 31756-2012 (ISO 6885:2006) Animal and vegetable fats and oils. Determination of the anisidine number

GOST 31933-2012 Vegetable oils. Methods for determining acid number

Note - When using this standard, it is advisable to check the validity of reference standards in the public information system - on the official website of the Federal Agency for Technical Regulation and Metrology on the Internet or according to the annual information index "National Standards", which was published as of January 1 of the current year, and on issues of the monthly information index "National Standards" for the current year. If the reference standard is replaced (modified), then when using this standard, you should be guided by the replacing (modified) standard. If the referenced standard is canceled without replacement, the provision in which the reference to it is given applies to the extent that this reference is not affected.

3 Terms and definitions

In this standard, the following terms are used with their respective definitions:

3.1 mesh: Presence in a transparent vegetable oil of individual tiny particles of waxes and wax-like substances that disappear when the oil is heated to 50 °C.

3.2 slight turbidity: The presence in vegetable oil of a continuous background of the smallest particles of waxes, wax-like and phosphorus-containing substances, which slightly reduce the transparency of the oil.

3.3 anisidine number number characterizing the content of secondary oxidation products (aldehydes) in vegetable oil

3.4 cold test

4 Classification

4.1 Sunflower oil, depending on processing, the level of values of quality indicators and purpose, is divided into grades in accordance with table 1.

Table 1

Sunflower oil brand	Purpose
Refined deodorized "Premium"	For direct consumption and for the production of children's and dietary products
Refined deodorized "Highest grade"	For direct consumption and for food production
Refined deodorized "First grade"
Refined non-deodorized	For food production 11 and for industrial processing
Unrefined "Top Grade" 2)	For direct consumption, for food production and for industrial processing
Unrefined "First grade" 2)
Unrefined for industrial processing	For industrial processing
r Pressing oil only. 2> Manufactured by pressing method only.

5 Technical requirements

5.1 Sunflower oil is produced in accordance with the requirements of this standard according to technological instructions and / or technological regulations approved 8 in the established order, using auxiliary means permitted by regulatory legal acts.
5.2 Characteristics
- 5.2.2 Microbiological parameters in Premium brand sunflower oil should not exceed the standards established for vegetable oil intended for the manufacture of baby food.
  5.2.3 Organoleptic and physico-chemical parameters must comply with the requirements specified in tables 2 and 3.

table 2

Table 3

Name of indicator	Norm for sunflower oil
refined deodorized	Refined non-dezo-dated	unrefined
	Top grade	First grade	Top grade	First grade	For industrial processing
frozen	inexhaustible	frozen	inexhaustible
Color number, mg iodine, no more
Acid number. mg KOH/g. no more
Mass fraction of non-fat impurities. %. no more	Absence
Mass fraction of phosphorus-containing substances. %, no more: in terms of stearoleolecithin in terms of Р?О 5	Absence
Soap (quality test)	Absence	Not standardized
Mass fraction of moisture and volatile substances. %. no more
Flash point of extraction oil. *C.not below	Not standardized		Not standardized
peroxide number. mole of active oxygen/kg. no more
Anisidine number, no more		Not standardized
cold test	Withstands the test	Not standardized	Withstands the test	Not standardized

5.2.4 Sunflower oil can be used for technical purposes. At the same time, specific norms of indicators are agreed with the consumer.

5.2.5 Identification characteristics

5.2.5.1 The fatty acid composition of sunflower oil and the method for its determination are given in Appendix A.
5.2.5.2 The norms and method for determining the indicator "mass fraction of unsaponifiable substances" are given in 8 Appendix B.

5.3 Requirements for raw materials

5.3.1 Sunflower oil is produced from sunflower seeds that meet the requirements of GOST 22391.

5.4 Marking

5.4.1 Each packaging unit of sunflower oil in a consumer container (label or package) is marked by any method that ensures its clear identification, indicating:

Product name;

Name and location of the manufacturer (address indicating the country of manufacture) or address of the organization authorized by the manufacturer to accept claims from purchasers;

Net weight and/or product volume;

Trademark of the manufacturer (if any);

Product brands;

Production dates (bottling dates for the packaged product);

Nutritional value (fat content in 100 g of oil);

Energy value of 100 g of the product, kcal (according to Appendix B);

Expiry date;

The designations of this standard;

Information on confirmation of conformity;

The date of manufacture (bottling date) of sunflower oil is applied in any way that ensures its clear reading.

5.4.2 Each unit of transport container with sunflower oil is marked with:

Name and location (legal address) of the manufacturer or packer;

Product name;

Product brand;

Net weight and number of consumer packaging units in a packaging unit for packaged oil or net weight of bulk oil;

Lot number and/or packing unit number;

Date of manufacture (date of pouring bulk sunflower oil in barrels, flasks, cisterns, tanks, containers or date of pouring packaged sunflower oil in consumer packaging);

Trademark of the manufacturer (if any);

Shelf life;

Names and designations of this standard;

Information about conformity assessment;

When grouped in shrink film, additional labeling characterizing the product is not required.

Open boxes for packing oil bottles are not labelled.

5.4.3 Handling signs “Keep out of sunlight”, “Keep out of moisture”, “Top” and “Fragile. Caution" is applied in accordance with GOST 14192.

Additional requirements for transport marking must comply with the terms of the contract for the supply of products.

5.4.4 When supplying sunflower oil for export, the marking must comply with the requirements of foreign trade organizations.

5.5 Packaging

5.5.1 Sunflower oil is produced packaged and bulk.
5.5.2 Sunflower oil is packaged by weight or volume in any consumer packaging made from materials approved for contact with vegetable oils in the prescribed manner. When packaging sunflower oil for baby food, it is necessary to additionally take into account the requirements established by regulatory legal acts in force in the territory of the state that adopted the standard.

Limits of permissible negative deviations of the net content from the nominal quantity according to GOST8.579.

5.5.3 Consumer containers with sunflower oil are hermetically sealed with caps, plugs or lids made of materials approved for contact with vegetable oils.

5.5.4 Consumer and shipping containers must ensure the safety of products and their compliance with the requirements (4) and this standard, including the indicators used for identification, during the entire shelf life, subject to the conditions of transportation and storage.

It is allowed to use imported containers and packaging materials approved for contact with vegetable oils.

5.5.5 Containers used for pouring and pouring sunflower oil must be clean, dry and free of foreign odors.

5.5.6 Sunflower oil intended for shipment to the Far North and equivalent areas is packaged in accordance with GOST 15846.

6 Environmental requirements

6.1 Control of maximum allowable concentrations (MPC) of harmful substances in the air is carried out in accordance with GOST 17.2.3.02 and with regulatory legal acts in force on the territory of the state that adopted the standard.
6.2 Soil protection from pollution by household and industrial waste is carried out in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.
6.3 Wastewater treatment, water consumption and water disposal in the production of sunflower oil is carried out in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.

7 Acceptance rules

7.1 Acceptance rules - according to GOST 5471.
7.2 Each batch of sunflower oil must be checked by the manufacturer's laboratory for compliance with the requirements of this standard and issued with a certificate of quality and safety.
7.3 Control over the content of toxic elements, pesticides, mycotoxins and radionuclides, as well as microbiological indicators of sunflower oil intended for baby food, is carried out in accordance with the procedure established by the product manufacturer and guaranteeing product safety.
7.4 The manufacturer guarantees compliance with the standards in terms of "cold test" and "anisidine number" on the basis of periodic analyzes carried out at least once a month.

8 Control methods

8.1 Sampling method - according to GOST 5471.
8.2 Determination of smell, color and transparency - according to GOST 5472.
8.3 Determination of taste - organoleptically.
8.4 Determination of the color number - according to GOST 5477.
8.5 Determination of acid number - according to GOST 5476, GOST 31933.
8.6 Determination of the mass fraction of non-fat impurities - according to GOST 5481.
8.7 Determination of the mass fraction of phosphorus-containing substances - according to GOST 31753.
8.8 Determination of the mass fraction of moisture and volatile substances - according to GOST 11812.
8.9 Determination of soap (qualitative sample) - according to GOST 5480.
8.10 Determination of flash point - according to GOST 9287.
8.11 Determination of peroxide number - according to GOST 26593.
8.12 Cold test - according to Appendix D.
8.13 Determination of the anisidine number - according to GOST 31756.
8.14 Preparation of samples for the determination of toxic elements - according to GOST 26929.
8.15 Determination of toxic elements - according to GOST 26927, GOST 26930, GOST 26932, GOST26933, GOST30178, GOST30538, GOST31628.
8.16 Determination of pesticides - according to the regulatory document in force in the territory of the state that adopted the standard.
8.17 Determination of mycotoxins - according to GOST 30711.
8.18 Determination of strontium-90, cesium-137 - according to the regulatory document in force on the territory of the state that adopted the standard.
8.19 Determination of microbiological indicators - according to the regulatory document in force in the territory of the state that adopted the standard.

9 Transport and storage

9.1 Sunflower oil is transported by all modes of transport in accordance with the requirements of the legislation on technical regulation and the terms of the contract for the supply of products.
9.2 Bulk sunflower oil is transported in 8 railway tanks equipped with a bottom discharge, in tank trucks with tight hatches and other covered vehicles in accordance with the requirements of the legislation on technical regulation and the terms of the contract for the supply of products.

When transporting by open vehicles, barrels, flasks and boxes with packaged sunflower oil must be protected from precipitation and sunlight.

9.3 Shipment of consumer containers with sunflower oil in open boxes must be agreed with the consumer.

9.4 Sunflower oil in consumer packaging, packed in corrugated cardboard boxes, grouped in shrink film, is transported in railway cars on pallets. The placement and fastening of boxes, transport packages and group packages must comply with the requirements of GOST 22477.

9.5 It is allowed to stack the boxes on pallets fixed on the walls of the car with the help of fasteners and wooden skids. The stacking height of boxes on pallets should not exceed five tiers.

9.6 Rail tank cars and tank trucks must comply with the requirements for the transport of food products.

Pouring sunflower oil intended for direct consumption into railway tanks and tank trucks is carried out using a pipeline reaching the bottom of the tank.

Sunflower oil packaged in consumer containers is stored in covered darkened rooms, in flasks and barrels - in covered areas.

10 Expiration dates

10.1 The shelf life of sunflower oil is set by the manufacturer depending on the production technology and storage conditions in accordance with the regulatory legal acts in force in the territory of the state that adopted the standard.

Annex A (informative)

Fatty acid composition of sunflower oil

A.1 The fatty acid composition of sunflower oil is given in Table A.1.

Table A.1

Determination of fatty acid composition - according to GOST 30418 and GOST 31663.

Annex B (informative)

Norms and method of control of the indicator "mass fraction of unsaponifiable substances" in sunflower oil

B.1 The norms and method of monitoring the indicator "mass fraction of unsaponifiable substances" in sunflower oil are given in Table B. 1.

Table B.1

Determination of the mass fraction of unsaponifiable substances - according to GOST 5479.

Calculation of the energy value of vegetable oil

The energy value, kcal / 100 g, is calculated by the formula Energy value \u003d 9 (100 - W-N).

The coefficient of energy value for fats, kcal / g - according to .

Mass fraction of moisture and volatile substances, %. - according to GOST 11812.

Mass fraction of non-fat impurities, %. - according to GOST 5481.

D.1 Glass bottles with sunflower oil are packed in wooden reusable boxes in accordance with GOST 10131 (N618.26.27) and GOST 11354, as well as plastic reusable boxes for bottles according to the document in accordance with which they are made, and corrugated cardboard boxes in accordance with GOST 13511 .

D.2 Packages with sunflower oil are packed in corrugated cardboard boxes No. 9 according to GOST 13511.

D.3 Bottles made of polymeric materials with sunflower oil are packed in corrugated cardboard boxes in accordance with GOST 9142 and GOST 13516 or other boxes according to the document in accordance with which they are made, ensuring the safety of products, or they are formed for packaging in shrink film in accordance with GOST 25951 or other a film with similar properties according to the document in accordance with which it is manufactured. Group packaging is formed using trays or pads made of corrugated cardboard in accordance with GOST 7376. or cardboard for consumer packaging in accordance with GOST 7933. or without gaskets. Roll packaging is carried out in accordance with the requirements of GOST 25776.

D.4 If necessary, products packed in shrink film are formed into bags on flat pallets in accordance with GOST 9078 or GOST 26381. To fasten the packages into a bag, polyethylene film is used in accordance with GOST 10354. steel tape in accordance with GOST 3560, polypropylene tape or stretch film according to the document according to which they are manufactured.

Palletizing is carried out in accordance with the requirements of GOST 22477, GOST 23285 and GOST 24597.

When forming transport packages using a shrink film, it is not allowed to weld it with a group packaging film.

D.5 Bulk sunflower oil is poured into aluminum flasks according to GOST 5037 with sealing rings made of oil-resistant rubber according to GOST 17133 and other materials approved for contact with vegetable oils in the prescribed manner, into non-galvanized steel barrels for foodstuffs according to GOST 13950, into barrels from polymeric materials permitted for contact with vegetable oils in the prescribed manner, into railway tanks and tankers, as well as, as agreed by the consumer, into other types of containers that ensure the safety of products and made from materials permitted for contact with vegetable oils in the prescribed manner.

Appendix D

(mandatory)

cold test

E.1 Scope

The method applies to vegetable oils and is intended to assess the effectiveness of the removal of waxes and wax-like substances during freezing.

E.2 Essence of the method

The method is based on determining the stability of the analyzed sample of the product to turbidity under the conditions established by this method.

E.3 Equipment and reagents

Glass according to GOST 25336 with a capacity of 400 cm 3.

Flask according to GOST 25336 with a capacity of 250 cm 3.

laboratory funnel according to GOST 25336 with a diameter of 100-110 mm.

Liquid glass thermometers in accordance with GOST 28498 with a division value of 1 ° C, allowing you to determine the temperature from 0'C to 150 ° C.

Electric stove according to GOST 14919 closed type.

Water bath providing temperature maintenance (2511) 'C.

Water bath with ice.

Filter paper according to GOST 12026.

Paraffin according to GOST 23683.

It is allowed to use other equipment with technical and metrological characteristics not worse and reagents in quality not lower than those indicated.

E.4 Preparation for determination

E.4.1 Sampling - according to GOST 5471.

E.5 Conducting a determination

E.5.1 In a glass according to GOST 25336 with a capacity of 400 cm 3, 200-300 cm 3 of the analyzed oil is filtered through a paper filter. A glass of a filtered oil sample is placed on an electric stove according to GOST 14919 and heated to (130 ± 1) °C with continuous stirring.

NOTE The purpose of preheating is to remove traces of moisture and destroy any centers of crystallization that may have persisted, as these may cause haze or premature crystallization.

When the temperature reaches (130 ± 1) °C, the heating is immediately stopped.

Hot oil is placed in a flask according to GOST 25336 with a capacity of 250 cm 3, filling it completely, closed with a stopper that ensures tightness, and thermostated in a water bath at a temperature of (2511) 9 C. When using a cork stopper, it is sealed with paraffin according to GOST 23683.

D.5.2 A flask with an analyzed oil sample, prepared according to D.5.1. placed in a water bath with ice so that the contents of the flask were completely covered with ice water, and incubated for 5.5 h at a temperature of 0 °C. periodically adding ice to maintain the specified temperature.

The test is considered positive if the analyzed oil sample is completely transparent (the test is passed).

If necessary, the test is continued for more than 5.5 hours. In this case, the analyzed oil sample is tested every hour. returning after each inspection to the ice water bath as quickly as possible. so that the oil temperature does not rise.

■ unrefined - 4 months;

Refined deodorized - 6 months;

Bulk -1.5 months.

E.2 The document confirming the eligibility of establishing expiration dates exceeding the minimum guaranteed ones can be an order of the head of the enterprise - the manufacturer of products, based on the data of the test report and the conclusion of the authorized bodies.

Bibliography

Technical regulation Customs Union TR TS 021/2011 "On food safety", approved by the Commission of the Customs Union dated 09.12/2011 No. 880'

Technical Regulations of the Customs Union TR TS 024/2011 "Technical Regulations for Oil and Fat Products", approved by the Commission of the Customs Union dated 09.12.2011 No. 883 3

Technical regulation of the Customs Union TR TS 022/2011 "Food products in terms of their labeling", approved by the Commission of the Customs Union dated 09.12.2011 No. 881'

Technical regulation of the Customs Union TR TS 005/2011 "On the safety of packaging". approved by Co 3 by the mission of the Customs Union dated August 16, 2011 No. 769 3

UDC 665.347.8:006.354 MKS 67.200.10 H62

Key words: sunflower oil, terms, grades, technical requirements, acceptance rules, control methods, labeling, packaging, transportation, storage, shelf life

Editor N.V. Talanov Technical editor O.N. Vlasova Proofreader I.A. Koroleva Computer imposition of IA. Naleikinoi

Handed over to the set 17.02.2014. Signed for publication on February 27, 2014. Format 60x84%. Arial headset.

Conv. oven l. 2.32. Uch.-ed. 1.70. Circulation 138 copies. Zach. 329.

GOST R 52901-2007 Corrugated cardboard for product packaging. Specifications.

GOST R 54463-2011 Containers made of cardboard and combined materials for food products. Specifications.

"1 GOST R 53228-2008 Scales of non-automatic action. Part 1. Metrological and technical requirements. Tests.

Valid on the territory of the member states of the Customs Union.

Published and printed in 123995 Moscow. Garnet lane. 4. www.goslinfo.ru

Interstate standard
Sunflower oil - specifications

GOST 1129-93

INTERSTATE STANDARD

FOREWORD

1 DEVELOPED MTK 238

INTRODUCED by Gosstandart of Russia

2 ADOPTED by the Interstate Council for Standardization, Metrology and Certification 1994-03-15 (report of the Technical Secretariat No. 1). Voted to accept:

3 INTRODUCED as state standard Ukraine by order of the State Standard of Ukraine dated 1996-06-19 No. 246 from 1997-01-01

4 INSTEAD OF GOST 1129-73

Introduction date 1996-01-01

Date of introduction in Ukraine 1997-01-01

This standard applies to sunflower oil obtained by pressing or extracting sunflower seeds.

Requirements for products aimed at ensuring their safety for the life and health of the population are set out in paragraphs 2.2.2 ("Peroxide number"), 2.2.4, 2.2.5, 2.3.2, 2.3.4, 4.2, 4.11-4.20

1.1 Depending on the method of processing and quality indicators, sunflower oil is divided into types, grades and brands indicated in table 1.

Table 1

Oil type
Sunflower oil, unrefined
Same
”
Sunflower oil hydrated
Same
”
Sunflower oil refined non-deodorized
Refined deodorized sunflower oil
Same

N o t e - Refined and hydrated sunflower oil sent for direct consumption (for delivery to trading network and to enterprises Catering) may be "frozen out".

1.2 For the production of children's and diet food Refined deodorized sunflower oil grade D.

1.3 Refined deodorized sunflower oil of grades P and D, as well as pressed sunflower oil: refined, non-deodorized, hydrated of the highest and first grades and unrefined of the highest and first grades are intended for delivery to the distribution network and to public catering establishments.

2 TECHNICAL REQUIREMENTS

2.1 Sunflower oil must be produced in accordance with the requirements of this standard according to technological instructions approved in the prescribed manner.

2.2 Characteristics

2.2.1 In terms of organoleptic characteristics, sunflower oil must meet the requirements specified in Table 2.

2.2.2 In terms of physical and chemical parameters, sunflower oil must meet the requirements specified in Table 3.

2.2.3 The names and norms of the reference indicators “Iodine number” and “Mass fraction of unsaponifiable substances” are given in Appendix 1.

2.2.4 The content of pesticides, toxic elements and mycotoxins in refined deodorized oil grades D and P, as well as in pressing oils intended for direct consumption (refined non-deodorized, hydrated premium and first grades, unrefined premium and first grades), should not exceed acceptable levels, established by biomedical requirements and sanitary standards for the quality of food raw materials and food products, approved by the Ministry of Health of the USSR on 01.08.89 No. 5061-89 (see Annexes 2 and 3).

table 2

Name of indicator	Oil characteristic
	refined		hydrated variety		unrefined oil
	deodorized	Undeodorized
Transparency	Transparent without sediment			Slight turbidity or "mesh" is not a rejection factor	The presence of a "grid" over the sediment is not a rejection factor.	Slight haze over sediment is not a rejection factor
Smell and taste	Without smell; the taste of an impersonal oil or with pleasant slightly specific shades of taste and smell for oil supplied to the distribution network and catering establishments	Peculiar to refined sunflower oil without foreign smell, taste and bitterness	Peculiar to sunflower hydrated oil without foreign smell, taste and bitterness		Peculiar to sunflower oil, without foreign smell, taste and bitterness	characteristic of sunflower oil. A slightly musty smell and a slight bitter taste are not a rejection factor.

N o t e

1 Slight turbidity and "grid" in refined and hydrated sunflower oil supplied for sale to the trade network and public catering establishments, as well as hydrated and refined oils for industrial processing is not a rejection factor (see Appendix 4).

2 In "frozen" refined and hydrated oils, "grid" is not allowed (see Appendix 4).

Table 3

Name of indicator	Oil standards
	refined			hydrated variety		unrefined variety
		deodorized brand	non-deodorized

Color number, mg iodine, no more								25	35
Acid number, mg KOH/g, no more								2,25	6,0
Mass fraction of non-fatty impurities, %, no more		Absence					0,05	0,10	0,20
Mass fraction of phosphorus-containing substances, %, not more than: in terms of stearoleolecithin		Absence						0,60	0,80
in terms of R202								0,053	0,070
Mass fraction of moisture and volatile substances,%, no more								0,20	0,30
Soap (quality test)		Absence		not defined
Flash point of extraction oil, 0С, not lower		234	225	225	225		225		225
Degree of transparency, fem, no more		25	25	40	-		40		---
Peroxide number, mmol/kg, no more than: freshly produced oil		5,0	5,0	5,0	---		5,0		---
after storage		10,0	10,0	10,0	---		10,0		---

N o t e

1 For "frozen" refined and hydrated oils sent to the distribution network and public catering establishments, the degree of transparency should be no more than 15 fem.

2 The indicator "Degree of transparency" is determined in oils sent for sale to the distribution network and public catering establishments, and in case of disagreement when assessing the organoleptic indicator "Transparency".

3 The sale of unrefined sunflower oil with an excess acid number must be agreed with the consumer.

2.2.5 Microbiological indicators in refined deodorized oil grade D should not exceed the permissible levels established by the biomedical requirements and sanitary standards for the quality of food raw materials and food products approved by the USSR Ministry of Health 01.08.89 No. 5061-89.

2.3 Requirements for raw materials

2.3.1 Sunflower oil must be produced from sunflower seeds that meet the requirements of GOST 22391 (except for seeds of the Pervenets variety).

For the production of refined deodorized oil of grade D, unrefined sunflower oil of at least the second grade must be used.

2.3.2 The content of pesticides in sunflower seed oil intended for the production of refined deodorized oil grade D, as well as refined non-deodorized, hydrated premium and first grades, unrefined premium and first grades used for direct consumption in food, should not exceed the permissible levels established medical and biological requirements and sanitary quality standards for food raw materials approved by the USSR Ministry of Health on 01.08.89 No. 5061-89 for oils for direct human consumption (see Appendix 2).

2.3.3 The content of pesticides in oil from sunflower seeds intended for the production of refined deodorized oil grade P, as well as refined non-deodorized, hydrated and unrefined oils used for processing into food products, should not exceed the permissible levels established by medical and biological requirements and sanitary quality standards for food raw materials and food products approved by the Ministry of Health of the USSR 01.08.89 No. 5061-89 for oils for processing into food products (see Appendix 2).

2.3.4 The content of toxic elements (Appendix 3) and mycotoxins in sunflower seeds intended for the production of refined deodorized oil grade D, as well as for oils for direct consumption, should not exceed the permissible levels established by biomedical requirements and sanitary standards quality of food raw materials and food products, approved by the Ministry of Health of the USSR 01.08.89 No. 5061-89.

2.4 Packing and pouring

2.4.1 Sunflower oil is produced packaged and bulk.

2.4.2 Sunflower oil is packaged:

Net weight 500 and 700 g in glass bottles according to GOST 10117, types VII and IX;

Net weight of 470, 575 and 1000 g in bottles of colored (or uncolored) polymeric materials approved for use by the state sanitary and epidemiological supervision;

Permissible deviations from the net weight in grams:

± 10 when packing 1000 g;

± 5 when packing from 470 to 750 g inclusive.

2.4.3 Bottles with sunflower oil should be hermetically sealed with an aluminum cap for sealing bottles with food liquids from aluminum foil according to GOST 745 with a cardboard sealing gasket with a cellophane coating.

Plastic bottles are sealed with polyethylene caps high pressure low density according to normative and technical documentation or brewed.

2.4.4 Bottles with sunflower oil are packed in wooden reusable boxes according to GOST 11354 and plastic reusable boxes for bottles according to normative documentation.

Bottles made of polymeric materials are also packed in corrugated cardboard boxes according to GOST 13516.

Packaging of bottles in wire reusable boxes in accordance with regulatory documentation, as well as in container-equipment in accordance with GOST 24831, is carried out only for local sale.

2.4.5 Bulk sunflower oil is packed in aluminum flasks according to GOST 5037 with sealing rings made of grease-resistant rubber according to GOST 17133 and other materials approved by the state sanitary and epidemiological supervision in accordance with the established procedure, in non-galvanized steel barrels for food products according to GOST 13950, and also, in agreement with the consumer, refined non-deodorized, hydrated and non-refined sunflower oil is poured into the consumer's container suitable for transporting vegetable oils by road.

Refined deodorized sunflower oil is poured into non-galvanized steel barrels for foodstuffs in accordance with GOST 13950, as well as in aluminum flasks in accordance with GOST 5037, only upon agreement with the consumer.

2.4.6 Sunflower oil is bottled according to types and grades.

2.4.7 Containers used for bottling sunflower oil must be clean, dry and free of foreign odors.

Barrels and flasks used for pouring refined deodorized sunflower oil must be thoroughly cleaned from the remnants of the oil stored in them, steamed, washed and dried.

2.4.8 Sunflower oil intended for shipment to the Far North and hard-to-reach areas must be packaged in accordance with GOST 15846.

2.5 Marking

2.5.1 Each bottle of sunflower oil must be affixed with a colorfully designed label, which is marked with:
- name of the manufacturer, its trademark;
- type, grade, brand of oil;
- net weight, g;
- date of bottling;
- fat content in 100 g of oil;
-calorie content of 100 g of the product (refined - 899 kcal, unrefined and hydrated - 898 kcal);
- guarantee period storage;

Marking by embossing is applied directly to a bottle made of polymeric materials.

The date of bottling of sunflower oil is affixed with a composter or a stamp on the label, embossed on the cap or in any other way that provides a clear indication, including laser.

When labeling bottles of oil subjected to "freezing", the name of the oil must be supplemented: "frozen".

2.5.2 Each packaging unit with oil is additionally marked with a label characterizing the product:
- the name of the manufacturer, its location and its trademark,
- type, grade and brand of oil;
- number of bottles per packaging unit or net weight for bulk oil;
- filling date for barrels and flasks or filling date for bottles;
- designation of this standard.

When marking boxes with oil that has been subjected to "freezing", the name of the oil must be supplemented: "frozen".

Box marking is not carried out when packing oil bottles in open boxes.

2.5.3 Marking of transport containers - in accordance with GOST 14192 with the application of manipulation signs “Keep away from heat” and “Keep away from moisture”.

3 ACCEPTANCE

3.1 Acceptance rules - according to GOST 5471.

3.2 Control over the content of pesticides, toxic elements, mycotoxins and microbiological indicators is carried out in accordance with the procedure established by the product manufacturer in agreement with the state sanitary and epidemiological supervision bodies and guaranteeing product safety.

4 TEST METHODS

4.1 Sampling method - according to GOST 5471.

4.2 Preparation of samples for the determination of toxic elements - according to GOST 26929.

4.3 Determination of smell, color and transparency - according to GOST 5472.

4.4 Determination of taste is carried out organoleptically.

4.5 Color number definition - according to GOST 5477.

4.6 Determination of acid number - according to GOST 5476.

4.7 Determination of the mass fraction of non-fat impurities and sludge - according to GOST 5481.

4.8 Determination of the mass fraction of phosphorus-containing substances - according to GOST 7824.

4.9 Determination of the mass fraction of moisture and volatile substances - according to GOST 11812.

4.10 Determination of soap (according to a qualitative sample) - according to GOST 5480.

4.11 Determination of flash point according to GOST 9287.

4.12 Determination of peroxide number - according to GOST 26593.

4.13 Determination of mercury - according to GOST 26927.

4.14 Determination of iron - according to GOST 26928.

4.15 Determination of arsenic - according to GOST 26930.

4.16 Determination of copper - according to GOST 26931.

APPENDIX I (informative)

Norms of indicators “Iodine number” and “Mass fraction of unsaponifiable substances” in sunflower oil

Name of indicator	Oil standards					Method of determination
	refined		hydrated variety	unrefined variety
	deodori- wrought brand	non-deodoro- roved

Iodine number g, J2/100 g					GOST 5475 (according to the Kaufman method)
Mass fraction of unsaponifiable substances, %, no more					GOST 5479

APPENDIX 2 (informative)

PERMISSIBLE LEVELS

APPENDIX 3 (informative)

PERMISSIBLE LEVELS

APPENDIX 4 (informative)

Terms used in this standard and explanations to them

INFORMATION DATA. REFERENCE REGULATIONS

	Application item number		Application item number
GOST 745-79	2.4.3	GOST 15846-79	2.4.8
GOST 5037-78	2.4.5	GOST 17133-83	2.4.6
GOST 5471-83	3.1; 4.1	GOST 21650-76	5.3
GOST 5472-50	4.3	GOST 22391-89	2.3.1
GOST 5475-69	Appendix 1	GOST 22477-77	5.3
GOST 5476-80	4.6	GOST 23285-78	5.3
GOST 6477-93	4.5	GOST 24597-81	5.3
GOST 6479-64	Appendix 1	GOST 24831-81	2.4.4
GOST 5480-59	4.10	GOST 26593-85	4.12
GOST 5481-89	4.7	GOST 26663-85	5.3
GOST 7824-80	4.8	GOST 26668-85	4.21
GOST 9218-86	5.1	GOST 26669-85	4.21
GOST 9225-84	4.21	GOST 26927-86	4.13
GOST 9287-59	4.11	GOST 26928-86	4.14
GOST 10117-91	2.4.2	GOST 26929-94	4.2
GOST 10444.12-88	4.21	GOST 26930-86	4.15
GOST 10674-82	5.1	GOST 26931-86	4.16
GOST 11812-66	4.9	GOST 26932-86	4.17
GOST 13516-86	2.4.4	GOST 26933-86	4.18
GOST 13950-91	2.4.5	GOST 26934-86	4.19
GOST 14192-77	2.5.3

Keywords: sunflower oil, types, technical requirements, acceptance, test methods, transportation and storage, manufacturer's guarantees.

Annex A (informative). Fatty acid composition of sunflower oil Appendix B (reference). Norms and method of control of the indicator "mass fraction of unsaponifiable substances" in sunflower oil Appendix B (recommended). Calculation of the energy value of vegetable oil Appendix D (recommended). Recommended shipping container Annex D (mandatory). Cold test Annex E (informative). Recommended shelf life of sunflower oil

Interstate standard GOST 1129-2013
"Sunflower oil. Specifications"
(put into effect by order of the Federal Agency for Technical Regulation and Metrology dated October 28, 2013 N 1253-st)

sunflower oil. Specifications

Foreword

The goals, basic principles and basic procedure for carrying out work on interstate standardization are established by GOST 1.0-92 "Interstate standardization system. Basic provisions" and GOST 1.2-2009 "Interstate standardization system. Interstate standards, rules and recommendations for interstate standardization. Rules for the development, adoption, application, renewal and cancellation

1 area of use

This standard applies to sunflower oil intended for direct human consumption, food production, including baby food, and industrial processing.

Requirements ensuring product safety - in 5.2.1-5.2.3, 5.3.2, product quality requirements - in 5.1, 5.2.3, 5.3.1, labeling requirements - in 5.4.

This standard uses normative references to the following interstate standards:

Table 1

Sunflower oil brand	Purpose
Refined deodorized "Premium"	For direct consumption and for the production of baby and dietary food
Refined deodorized "High grade"	For direct consumption and for food production
Refined deodorized "First grade"	For direct consumption and for food production
Refined non-deodorized	For food production and industrial processing
Unrefined "Highest grade"	For direct consumption, for food production and for industrial processing
Unrefined "First grade"
Unrefined for industrial processing	For industrial processing
* Pressing oil only. ** Produced by pressing only.

5 Technical requirements

5.1 Sunflower oil is produced in accordance with the requirements of this standard according to technological instructions and / or technological regulations approved in the prescribed manner, using auxiliary means permitted by regulatory legal acts.

5.2 Characteristics

5.2.2 Microbiological parameters in "Premium" brand sunflower oil should not exceed the standards established for vegetable oil intended for the manufacture of baby food.

5.2.3 Organoleptic and physico-chemical parameters must comply with the requirements specified in tables 2 and .

table 2

Name of indicator	Characteristics of sunflower oil
	refined				unrefined
	deodorized			undeodorized	Top grade	First grade	For industrial processing
		Top grade	First grade
Transparency	Transparent without sediment			Slight turbidity or "grid" is allowed		Sediment and slight turbidity or "mesh" over the sediment is allowed	Not standardized
Smell and taste	Odorless, impersonal taste			Peculiar to sunflower oil, without foreign smell and taste

Table 3

Name of indicator	Norm for sunflower oil
	refined deodorized					Refined non-deodorized	unrefined
		Top grade		First grade			Top grade	First grade	For industrial processing
		frozen	unfrozen	frozen	unfrozen
Color number, mg iodine, no more
Acid number, mg KOH/g, no more
Mass fraction of non-fatty impurities, %, no more	Absence
Mass fraction of phosphorus-containing substances, %, not more than:	Absence
in terms of stearoleolecithin
in terms of
Soap (quality test)	Absence						Not standardized
Mass fraction of moisture and volatile substances,%, no more
Flash point of extraction oil, °C, not below	Not standardized						Not standardized
Peroxide number, mole of active oxygen/kg, no more
Anisidine number, no more				Not standardized
cold test	Withstands the test		Not standardized	Withstands the test	Not standardized

5.2.4 Sunflower oil can be used for technical purposes. At the same time, specific norms of indicators are agreed with the consumer.

5.3 Requirements for raw materials

5.4 Marking

5.4.1 Each packaging unit of sunflower oil in a consumer container (label or package) is marked by any method that ensures its clear identification, indicating:

Product name;

Name and location of the manufacturer (address indicating the country of manufacture) or address of the organization authorized by the manufacturer to accept claims from purchasers;

Net weight and/or product volume;

Trademark of the manufacturer (if any);

Product brands;

Production dates (bottling dates for the packaged product);

Nutritional value (fat content in 100 g of oil);

Energy value of 100 g of the product, kcal (according to Appendix B);

Expiry date;

The designations of this standard;

Information on confirmation of conformity;

The date of manufacture (bottling date) of sunflower oil is applied in any way that ensures its clear reading.

5.4.2 Each unit of transport container with sunflower oil is marked with:

Name and location (legal address) of the manufacturer or packer;

Product name;

Product brand;

Net weight and number of consumer packaging units in a packaging unit for packaged oil or net weight of bulk oil;

Lot number and/or packing unit number;

Date of manufacture (date of pouring bulk sunflower oil in barrels, flasks, cisterns, tanks, containers or date of pouring packaged sunflower oil in consumer packaging);

Trademark of the manufacturer (if any);

Shelf life;

Names and designations of this standard;

Information about conformity assessment;

When grouped in shrink film, additional labeling characterizing the product is not required.

Open boxes for packing oil bottles are not labelled.

5.4.3 Handling signs "Protect from sunlight", "Protect from moisture", "Top" and "Fragile. Caution" are applied in accordance with GOST 14192.

Additional requirements for transport marking must comply with the terms of the contract for the supply of products.

5.4.4 When supplying sunflower oil for export, the marking must comply with the requirements of foreign trade organizations.

5.5 Packaging

5.5.1 Sunflower oil is produced packaged and bulk.

Limits of permissible negative deviations of the net content from the nominal quantity according to GOST 8.579.

5.5.3 Consumer containers with sunflower oil are hermetically sealed with caps, plugs or lids made of materials approved for contact with vegetable oils.

5.5.4 Consumer and shipping containers must ensure the safety of products and their compliance with the requirements of this standard, including the indicators used for identification, during the entire shelf life, subject to the conditions of transportation and storage.

The recommended shipping container for packaging sunflower oil is given in Appendix D. It is allowed to use imported containers and packaging materials approved for contact with vegetable oils.

5.5.5 Containers used for pouring and bottling sunflower oil must be clean, dry and free from foreign odors.

5.5.6 Sunflower oil intended for shipment to the regions of the Far North and areas equivalent to them are packed according to

1129 sunflower oil specifications.

Delivery methods

This GOST is in:

Organizations:

sunflower oil. Specifications

Normative references

SUNFLOWER OIL

Specifications

Foreword

About the standard

9 Transport and storage

Annex A (informative)

Annex B (informative)

Norms and method of control of the indicator "mass fraction of unsaponifiable substances"

in sunflower oil

GOST 1129-2013

INTERSTATE STANDARD

SUNFLOWER OIL Specifications

1 area of ​​use

2 Normative references

5.4 Marking

5.5 Packaging

6 Environmental requirements

7 Acceptance rules

8 Control methods

SUNFLOWER OIL

Specifications

1 area of use